Barry, E. F. & Grob, R. L.
Columns for Gas Chromatography
Performance and Selection
John Wiley & Sons 2007.4
298 pp. (H)
ISBN 0-471-74043-8
12,400円
Contents
Preface. Acknowledgments. 1 Introduction. Evolution of Gas Chromatographic Columns. Central Role Played by the Column. Justification for Column Selection and Care. Literature on Gas Chromatographic Columns. Gas Chromatographic Resources on the Internet. References. 2 Packed Column Gas Chromatography. Introduction. Solid Supports and Adsorbents. Stationary Phases. Column Preparation. United States Pharmacopeia and National Formulary Chromatographic Methods. References. 3 Capillary Column Gas Chromatography. Introduction. Capillary Column Technology. Preparation of Fused-Silica Capillary Columns. Chromatographic Performance of Capillary Columns. Stationary-Phase Selection for Capillary Gas Chromatography. Specialty Columns. Capillary Column Selection. Column Installation and Care. Special Gas Chromatographic Techniques. References. 4 Column Oven Temperature Control. Thermal Performance Variables and Electronic Considerations. Advantages of Temperature Programming over Isothermal Operation. Oven Temperature Profiles for Programmed-Temperature Gas Chromatography. Role of Computer Assistance in Optimizing Separations in Gas Chromatography. Fast or High-Speed Gas Chromatography. Subambient Oven Temperature Control. References. Selected References. Appendix A: Guide to Selection of Packed Columns. Appendix B: Column Selection. Index. *
Nicolay, X. ed.
Odors In the Food Industry
食品産業の臭気
Springer-Verlag 2006.10
162 pp. (H)
ISBN 0-387-33510-2
17,000円
Contents
1.Odor Problem in the Food Industry.- 2.Odor Measurements.- 3.The Application of Intelligent Sensor Array for Air Pollution Control in the Food Industry.- 4.Preconcentration Prior to Gas Chromatography.- 5.Electronic-Nose Technology: Application for Quality Evaluation in the Fish Industry.- 6.Odor Prevention in the Food Industry.- 7.Odor Treatment: Physico-Chemical Technologies.- 8.Odor Treatment: Biological Technologies.- Index/ *
Pfleger, K. et al.
Mass Spectral and GC Data of Drugs, Poisons, Pesticides, Pollutants and Their Metabolites 3rd ed.
薬物・毒物・農薬・汚染物質とその代謝産物の質量スペクトルとガスクロマトグラフィーデータ 第3版
John Wiley & Sons 2007.5
1800 pp. (H)
ISBN 3-527-31538-1
98,600円
Contents
* 本書は臨床サンプルから20年以上にわたって集められた、有害物質の質量スペクトルとガスクロマトグラフィーのデータ集です。単なる鎮痛剤から合成麻薬まで、そして農薬から化学兵器まで7,500種類の有害物質を網羅しています。またこれらの物質は通常、人間の体内で分解されますが、本書はその代謝物も含めて収録しており、その代謝物から元々の物質を同定することを可能にしています。未知の物質の同定において、まず使われるのが分子量であることから、本書は収録する物質のスペクトルを分子量順に配列しています。
VOLUME 1: METHODS, TABLES, INDEXES Experimental methods Userユs guide Tables of compounds in the atlas listed by - name - chemical category CAS number index
VOLUME 2: SPECTRA contains 7500 unique spectra in order of molecular mass data given for each substance: - full MS spectrum including base peak and characteristic masses - structural formula, empirical formula and exact mass - GC retention index and detection methods - compound category and sample type - CAS registry number - compound names (up to four) *
Guochon, G. et al.
Fundamentals of Preparative and Nonlinear Chromatography 2nd ed.
Academic Press 2006.4
990 pp.(H)
ISBN 0-12-370537-1
40,500円
Contents
1. Introduction, Definitions, Goal/ 2. The Mass Balance Equation of Chromatography and Its General Properties/ 3. Single-Component Equilibrium Isotherms/ 4. Competitive Equilibrium Isotherms/ 5. Transfer Phenomena in Chromatography/ 6. Linear Chromatography/ 7. Band Profiles of Single-Components with the Ideal Model/ 8. Band Profiles of Two Components with the Ideal Model/ 9. Band Profiles in Displacement Chromatography with the Ideal Model/ 10. Single--Component Profiles with the Equilibrium Dispersive Model/ 11. Two-Component Band Profiles with the Equilibrium-Dispersive Model/ 12. Frontal Analysis, Displacement and the Equilibrium-Dispersive Model/ 13. System Peaks with the Equilibrium-Dispersive Model/ 14. Kinetic Models and Single-Component Problems/ 15. Gradient Elution Chromatography under Nonlinear Conditions/ 16. Kinetic Models and Multicomponent Problems/ 17. Simulated Moving Bed Chromatography/ 18. Optimization of the Experimental Conditions/
* The second edition of Fundamentals of Preparative and Nonlinear Chromatography is devoted to the fundamentals of a new process of purification or extraction of chemicals or proteins widely used in the pharmaceutical industry and in preparative chromatography. This process permits the preparation of extremely pure compounds satisfying the requests of the US Food and Drug Administration. The book describes the fundamentals of thermodynamics, mass transfer kinetics, and flow through porous media that are relevant to chromatography. *
Funk, W. et al.
Quality Assurance in Analytical Chemistry 2nd ed.
Applications in Environmental, Food and Materials Analysis, Biotechnology, and Medical Engineering
Wiley-VCH 2007.1
277 pp. (H)
ISBN 3-527-31114-9
15,600円
Contents
Preface / List of Symbols / Introduction. 1 General Differentiation of Analytical Processes / 2 Quality of Analytical Processes and Results / 3 The System of Analytical Quality Assurance / 4 The Four-Phase Model of Analytical Quality Assurance / Part 1 Phase I: Establishing a New Analytical Procedure. 1 Introduction / 2 Calibration of the Fundamental Analytical Procedure / 3 Analyses at Very Low Concentrations / 4 Validation of Individual Process Steps and Examination of Matrix Influences / 5 Additional Statistical Methods / 6 Use of Internal Standards / 7 Preparing for Routine Analysis / 8 Summary of the Results of Phase I (Process Development): Documentation / Part 2 Phase II: An Analytical Process Becomes Routine; Preparative Quality Assurance. 1 Introduction / 2 Selection of the Analytical Procedure / 3 The “Training” Phase of the Process / 4 Establishment of Quality Objectives to be Adhered to in Routine Usage / 5 Control Samples for Internal Quality Assurance / 6 The Control Chart System / Part 3 Phase III: Routine Quality Assurance. 1 Introduction / 2 Fundamental Measures of Internal Quality Assurance / 3 Routine Quality Control / 4 Special Quality Problems in Routine Analysis / 5 Corrective Measures / 6 Documentation and Archiving / Part 4 Phase IV: External Analytical Quality Assurance. 1 Introduction / 2 Audits / 3 Interlaboratory (or Round Robin) Tests / 4 Effects of Internal Quality Assurance on the Results of Interlaboratory Tests / 5 Conclusion / Part 5 Definitions. 1 Quality and Quality Management / 2 Analytical Terms / 3 Analytical Results / 4 Deviation, Uncertainty / 5 Materials, Samples / 6 Statistical Tests / 6 References. Appendix / Subject Index. *
Danzer, K.
Analytical Chemistry
Theoretical and Metrological Fundamentals
Springer-Verlag 2007.1
315 pp. (H)
ISBN 3-540-35988-5
13,900円
Contents
Symbols / Abbreviations and Acronyms / 1 Object of Analytical Chemistry / 2 The Analytical Process / 3 Signals in Analytical Chemistry / 4 Statistical Evaluation of Analytical Results / 5 Studying In uences and Optimizing Analytical Procedures / 6 Calibration in Analytical Chemistry / 7 Analytical Performance Characteristics / 8 Presentation, Interpretation and Validation of Analytical Results / 9 Assessment of Analytical Information / Glossary of Analytical Terms / References / Index. **
* Fundamentals of Analytical Chemistry are usually presented as a sum of chemical and physical foundations, laws, axioms and equations for analytical methods and procedures. In contrast, this book delivers a practice-oriented, general guiding theory valid for all methods and techniques. Starting with a closer look to analytical signals and their dependencies, all the important figures of merit characterizing the power of analytical procedures and the reliability of analytical results are discussed and quantified, such as sensitivity, precision, accuracy and ruggedness. *
779-7 登録日 07.10.08